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TECHNOLOGICAL WATCH

Type of information: TECHNICAL ARTICLES

In this section, you can access to the latest technical information related to the PISA project topic.

Cycloaddition of nitrile imines to graphene: a theoretical and experimental approach

Density functional theory (DFT) studies of the interaction between graphene sheets and nitrile oxides have proved the feasibility of the reaction via 1,3?dipolar cycloaddition. The viability of the approach has been also confirmed experimentally through the cycloaddition of few?layer exfoliated graphene and nitrile oxides containing functional organic groups with different electronic nature. The cycloaddition reaction has been successfully achieved in one pot from the corresponding oximes under microwave (MW) irradiation. The successful formation of the isoxazoline ring has been confirmed by Raman spectroscopy, Fourier?transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA) and X?Ray photoelectron spectroscopy (XPS).

» Author: Helena Uceta, Maria Vizuete, Jose R Carrillo, Myriam Barrejon, Jos? Luis G Fierro, Pilar Prieto, Fernando Langa

» Reference: doi:10.1002/chem.201903105

» Publication Date: 19/08/2019

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